Tube-type vacuum high-temperature sintering furnace

Column:High temperature sintering furnace

Date:2025-11-05

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Desc:Tube-type vacuum high-temperature sintering furnace

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The tubular high-temperature vacuum sintering furnace is a key equipment for high-temperature sintering and heat treatment of materials in a vacuum or specific atmosphere environment. It is widely used in fields such as materials science, metallurgy, electronics, chemical industry, and new energy. The following is a detailed introduction about it: Working principle Vacuum environment creation: Use vacuum equipment such as mechanical pumps, diffusion pumps or molecular pumps to pump the air in the furnace to a high vacuum, usually 10⁻¹Pa to 10⁻⁵Pa. A low pressure environment can inhibit the oxidation reaction of the material and promote the escape of gas impurities inside the material. For example, vacuum degassing during ceramic sintering can reduce the porosity and increase the density of the green body to more than 95%.  High-temperature sintering: Using heating elements such as resistance wires, silicon carbon rods, silicon-molybdenum rods or graphite heating elements, the temperature in the furnace is raised to the target value, which generally covers 100°C to 1800°C. The heating element converts electrical energy into thermal energy, forming an axially uniform temperature field in the furnace tube through thermal radiation, causing the powder particles in the material to melt and combine with each other to form dense blocks or parts.  Atmosphere control: According to process requirements, inert gases, such as argon, nitrogen, or reducing gases, such as hydrogen, ammonia, etc., can be introduced into the furnace tube to form a protective atmosphere or participate in chemical reactions. For example, when preparing metal powder, hydrogen can reduce metal oxides to obtain high-purity metal powder.  Structural composition: Furnace body: generally welded by section steel and steel plates, with alumina fiber and other insulation materials filled in the middle to reduce heat loss. The furnace body can adopt a double-layer furnace shell structure, and a fan is installed between the outer furnace shells to achieve rapid temperature rise and cooling.  Furnace tube: usually made of high-temperature resistant 310S stainless steel tube, quartz tube or corundum tube, etc., with stainless steel flanges at both ends for sealing and connecting the vacuum system, gas introduction system, etc., to facilitate the entry and exit of materials.  Heating elements: According to different temperature requirements, high-temperature iron-chromium-aluminum, silicon-molybdenum rods, silicon-carbon rods, etc. can be selected as heating elements. They are generally wound into spirals or other shapes and placed in the furnace lining to heat the circumference of the furnace tube.  Vacuum system: It consists of mechanical pumps, diffusion pumps, molecular pumps, vacuum valves, vacuum pipelines and vacuum measuring instruments. It is used to extract the air in the furnace to obtain the required vacuum degree.  Control system: Using technologies such as PID adjustment and fuzzy control, it can achieve precise control of parameters such as temperature, vacuum degree, and atmosphere. Usually equipped with a touch screen or control panel, the operator can easily set and monitor the sintering process parameters.  Technical features: Good high-temperature stability: It can operate stably in high temperature environments to meet the preparation needs of different materials. The maximum temperature of some tubular high-temperature vacuum sintering furnaces can reach 1800°C.  Precise temperature control: The temperature inside the furnace is evenly distributed. It adopts an advanced temperature control system and the temperature control accuracy can reach ±1℃, ensuring that the materials are heated evenly and improving product quality.  Flexible atmosphere control: The atmosphere in the furnace can be accurately adjusted according to process requirements, and is suitable for sintering experiments of materials that are sensitive to atmosphere.  Energy saving and environmental protection: Using electric heating method, combined with efficient insulation materials, the energy utilization rate is high and the outer surface temperature is low, which reduces energy consumption and environmental pollution.  Application fields Materials research: widely used in the preparation and research of ceramics, metals, semiconductors, nanomaterials, etc., such as sintering of ceramics, smelting and heat treatment of metals, preparation of semiconductor materials, etc.  Electronic industry: used to manufacture semiconductor devices, electronic components, integrated circuits, etc., such as thin film deposition, surface treatment and other processes.  Chemical industry: often used in the synthesis of polymer materials, activation of catalysts, heating of chemical reactions, etc.  Metallurgical industry: Mainly used in metal refining, continuous casting and other processes. Through precise control of temperature and time, efficient metal smelting and production of high-quality products are achieved.